| 卷烟烟气总粒相物中氟节胺含量的检测方法 |
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| 引用本文： | 吴娜,夭建华,叶艳青,黄海涛,米其利.卷烟烟气总粒相物中氟节胺含量的检测方法[J].分析测试学报,2011,30(2):213-217. |
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| 作者姓名： | 吴娜 夭建华 叶艳青 黄海涛 米其利 |
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| 作者单位： | 云南烟草科学研究院烟用添加剂安全测试中心;云南民族大学化学与生物技术学院; |
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| 基金项目： | 中烟公司资助项目(2007JC01) |
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| 摘 要： | 建立了气相色谱电子捕获器法检测卷烟抽吸过程中氟节胺向主流烟气总粒相物中转移量的方法,卷烟在标准条件下抽吸,用剑桥滤片捕集主流烟气总粒相物,经乙腈提取、石墨碳黑固相萃取柱或自制混合层析柱净化、GC/ECD检测后,外标法定量.氟节胺在0.02 ～20 mg/L范围内线性关系良好,检出限为9.14×10-6 g/L.加标量为...
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| 关 键 词： | 主流烟气总粒相物 石墨碳黑固相萃取柱 自制混合层析柱 氟节胺 转移量 气相色谱 |
Determination of Amount of the Flumetralin in Total Particulate Matter of Mainstream Cigarette Smoke |
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| WU N,YAO Jian hu,YE Yan qing,HUANG Hai tao,MI Qi li.Determination of Amount of the Flumetralin in Total Particulate Matter of Mainstream Cigarette Smoke[J].Journal of Instrumental Analysis,2011,30(2):213-217. |
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| Authors: | WU N YAO Jian hu YE Yan qing HUANG Hai tao MI Qi li |
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| Institution: | WU Na1,2,YAO Jian-hua1,YE Yan-qing2,HUANG Hai-tao 1,MI Qi-li1(1.Research and Develop ment Center for Safety Determination of Tobacco Additives,Yunnan Academy of Tobacco Science,Kunming 650106,China,2.School of Chemistry and Biotechnology,Yunnan University of Nationnalities,Kunming 650500,China) |
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| Abstract: | A gas chromatographic method coupled with electron capture detection(GC/ECD) was developed for the determination of flumetralin deliver amount in total particulate matter(TPM) of mainstream cigarette smoke during cigarette smoking.Under the standard conditions,cigarette were smoked to collect the TPM of mainstream cigarette smoke with cambridge filter,and then extracted with acetonitrile.The extracts were cleaned up with the SupelcleanTM ENVITM-Carb SPE tubes or the mixed chromatography column,and determine... |
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| Keywords: | TPM of mainstream cigarette smoke SupelcleanTM ENVITM-Carb SPE tubes mixed chromatography column flumetralin deliver amount gas chromatography |
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