| ASE/GC-MS法同时测定海洋沉积物中65种多氯联苯、多环芳烃与有机氯农药 |
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| 引用本文： | 贺行良,夏宁,张媛媛,王江涛. ASE/GC-MS法同时测定海洋沉积物中65种多氯联苯、多环芳烃与有机氯农药[J]. 分析测试学报, 2011, 30(2): 152-160. DOI: 10.3969/j.issn.1004-4957.2011.02.007 |
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| 作者姓名： | 贺行良 夏宁 张媛媛 王江涛 |
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| 作者单位： | 国土资源部海洋油气资源与环境地质重点实验室;青岛海洋地质研究所;中国海洋大学海洋化学理论与工程技术教育部重点实验室; |
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| 基金项目： | 国土资源部海洋油气资源与环境地质重点实验室基金资助项目(RME200918) |
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| 摘 要： | 建立了加速溶剂萃取/气相色谱-质谱法(ASE/GC-MS)同时测定海洋沉积物中28种多氯联苯(PCBs)、16种多环芳烃(PAHs)和21种有机氯农药(OCPs)的分析方法.结果表明,ASE的最佳萃取温度为100 ℃,最佳静态时间为5 min.GC-MS同时分析65种化合物时,PAHs的线性范围为0.05 ～5.00 ...
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| 关 键 词： | 海洋沉积物 多氯联苯 多环芳烃 有机氯农药 同时测定 |
Simultaneous Determination of 65 Polychlorinated Biphenyls,Polycyclic Aromatic Hydrocarbons and Organochlorine Pesticides in Marine Sediments by GC-MS with Accelerated Solvent Extraction |
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| HE Xing liang,XIA Ning,ZHANG Yuan yuan,WANG Jiang tao. Simultaneous Determination of 65 Polychlorinated Biphenyls,Polycyclic Aromatic Hydrocarbons and Organochlorine Pesticides in Marine Sediments by GC-MS with Accelerated Solvent Extraction[J]. Journal of Instrumental Analysis, 2011, 30(2): 152-160. DOI: 10.3969/j.issn.1004-4957.2011.02.007 |
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| Authors: | HE Xing liang XIA Ning ZHANG Yuan yuan WANG Jiang tao |
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| Affiliation: | HE Xing-liang1,2,3,XIA Ning1,ZHANG Yuan-yuan2,WANG Jiang-tao3(1.Key Laboratory of Marine Hydrocarbon Resources and Environmental Geology,Ministry of Land and Resources,Qingdao 266071,China,2.Qingdao Institute of Marine Geology,3.Key Laboratory of Marine Chemistry Theory and Technology,Ministry of Education,Ocean University of China,Qingdao 266100,China) |
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| Abstract: | |
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| Keywords: | marine sediments polychlorinated biphenyls polycyclic aromatic hydrocarbons or-ganochlorine pesticides simultaneous determination |
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