Molecular and crystal structure of 1,2-dihydro-3H-1,3,4-benzotriazepines |
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Authors: | Yu M Chumakov Yu A Simonov G Bocelli M Gdaniec S V Vlassiuk V I Pavlovsky |
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Institution: | (1) Institute of Applied Physics of Academy of Sciences of Moldova, Kishinev, MD-2028, Moldavian Republic;(2) IMEM-CNR, I-43100 Parma, Italy;(3) Chemistry Faculty, A. Mickiewicz University, 60-780 Poznan, Poland;(4) A. V. Bogatsky Physico-Chemical Institute, Ukraine National Academy of Sciences, Odessa, 270080 |
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Abstract: | Three novel 1,2-dihydro-3H-1,3,4-benzotriazepines have been synthesized: 7-bromo-5-phenyl-3-phenylcarbamoyl-1,2-dihydro-3H-1,3,4-benzotriazepin-2-one,
7-bromo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin-2-thione, and 7-methyl-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin-2-one.
Their crystal structures have been determined using X-ray analysis.
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 7, pp. 1048–1056, July, 2006. |
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Keywords: | benzotriazepine hydrogen bonds crystal structure X-ray analysis |
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