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Molecular and crystal structure of 1,2-dihydro-3H-1,3,4-benzotriazepines
Authors:Yu M Chumakov  Yu A Simonov  G Bocelli  M Gdaniec  S V Vlassiuk  V I Pavlovsky
Institution:(1) Institute of Applied Physics of Academy of Sciences of Moldova, Kishinev, MD-2028, Moldavian Republic;(2) IMEM-CNR, I-43100 Parma, Italy;(3) Chemistry Faculty, A. Mickiewicz University, 60-780 Poznan, Poland;(4) A. V. Bogatsky Physico-Chemical Institute, Ukraine National Academy of Sciences, Odessa, 270080
Abstract:Three novel 1,2-dihydro-3H-1,3,4-benzotriazepines have been synthesized: 7-bromo-5-phenyl-3-phenylcarbamoyl-1,2-dihydro-3H-1,3,4-benzotriazepin-2-one, 7-bromo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin-2-thione, and 7-methyl-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin-2-one. Their crystal structures have been determined using X-ray analysis. __________ Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 7, pp. 1048–1056, July, 2006.
Keywords:benzotriazepine  hydrogen bonds  crystal structure  X-ray analysis
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