Solvothermal synthesis of Cd(OH)2 and CdO nanocrystals and application as a new electrochemical sensor for simultaneous determination of norfloxacin and lomefloxacin |
| |
| Authors: | Lotf Ali Saghatforoush Soheila Sanati Robabeh Mehdizadeh Mohammad Hasanzadeh |
| |
| Institution: | 1. Department of Chemistry, Payam Noor University, Tehran, Iran;2. Drug Applied Research Center, Tabriz University of Medical Sciences, Tabriz, Iran;3. Liver and Gastrointestinal Diseases Research Center, Tabriz University of Medical Sciences, Tabriz 51664, Iran |
| |
| Abstract: | Cadmium hydroxide (Cd(OH)2) microcrystals were synthesized in ethanol–water medium by using cadmium chloride as cadmium source and 1,10-phenanthroline as complexation agent under solvothermal condition. The sample was characterized by FT-IR, X-ray diffraction (XRD), scanning electron microscopy (SEM) and TEM. The as-prepared Cd(OH)2 product were transformed to hexagonal CdO nanocubes by thermal treatment in air at 500 °C. The possible growth mechanism for the formation of different morphologies at basic medium has been proposed. DPV experiments were carried out for the simultaneous determination of norfloxacin and lomefloxacin in the acetate buffer solution with pH 4.5. |
| |
| Keywords: | Cadmium hydroxide 1 10-Phenanthroline Cadmium oxide Nanocube |
| 本文献已被 ScienceDirect 等数据库收录！ |
|
