A novel cyclization reaction of oxido diazoalkanes: formation of 1-substituted cycloalkenes |
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| Affiliation: | 1. Department of Nanotechnology, CPGS, Visvesvaraya Technological University, Muddenahalli, Karnataka 562101, India;2. Centre for Material Science, University of Mysore, Mysore, Karnataka 570006, India;3. Adichunchanagiri Institute for Molecular Medicine, AIMS, Adichunchanagiri University, BG Nagara 571448, Karnataka 02, India;4. Department of Chemistry, Govt. S. K. S. J. Technological Institute (Affiliated to Visvesvaraya Technological University), K R Circle, Bangalore, Karnataka 560001, India;5. Faculty of Natural Sciences, Adichunchanagiri University, BG Nagara 571448, Karnataka, India;6. Department of Chemistry, Maharani’s Science College for Women, Palace Road, Bangalore, Karnataka 560001, India;7. Division of Natural Science Northwest Mississippi Community College, University of Mississippi Campus, Desoto Centre, Southaven, MS 38671, USA;8. Institution of Excellence, University of Mysore, Manasagangotri, Mysore, Karnataka 570006, India;1. Department of Medicinal Chemistry, Key Laboratory of Drug-Targeting and Drug Delivery System of the Education Ministry and Sichuan Province, Sichuan Engineering Laboratory for Plant-Sourced Drug and Sichuan Research Center for Drug Precision Industrial Technology, West China School of Pharmacy, Sichuan University, Chengdu 611041, China;2. Precision Pharmacy & Drug Development Center, Department of Pharmacy, Tangdu Hospital, Fourth Military Medical University, Xi’an 710038, China;3. Institute of Traditional Chinese Medicine Pharmacology and Toxicology, Sichuan Academy of Chinese Medicine Sciences, Chengdu 610041, China;1. Organometallics and Nanomaterials, Department of Chemistry, University of the Western Cape, Private Bag X17, Bellville 7535, South Africa;2. School of Physical Sciences, Jomo Kenyatta University of Agriculture and Technology, P.O. Box 62, 000-00200 Nairobi, Kenya;3. Department of Science and Innovation/Mintek Nanotechnology Innovation Centre (DSI/Mintek NIC), Biolabels Node, Department of Biotechnology, University of the Western Cape, Private Bag X17, Bellville 7535, South Africa;4. Department of Chemistry, Rutgers, The State University of New Jersey, Newark, NJ 07102, United States;1. Department of Chemistry and Biochemistry, The Ohio State University, Columbus, OH 43210, USA |
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| Abstract: | The thermal decomposition of dialkali metal salts of δ-hydroxybutyl ketone and ε-hydroxypentyl ketone tosylhydrazones in diglyme at 80–120 °C produced the 1-substituted cyclopentene and cyclohexene, respectively. |
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