| C18-MCM-41新型涂层在固相微萃取中的应用 |
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| 引用本文： | 侯经国,田锐,马骞,杜新贞,高锦章. C18-MCM-41新型涂层在固相微萃取中的应用[J]. 化学研究与应用, 2005, 17(5): 700-702 |
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| 作者姓名： | 侯经国 田锐 马骞 杜新贞 高锦章 |
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| 作者单位： | 西北师范大学化学化工学院,甘肃,兰州,730070;西北师范大学化学化工学院,甘肃,兰州,730070;西北师范大学化学化工学院,甘肃,兰州,730070;西北师范大学化学化工学院,甘肃,兰州,730070;西北师范大学化学化工学院,甘肃,兰州,730070 |
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| 基金项目： | 西北师范大学科技创新工程资助项目 |
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| 摘 要： | 固相微萃取（SPME）是集采样、萃取和富集于一体的样品前处理技术，该技术于1990年由Pawliszyn提出。由于其不使用有机溶剂，且简便、快速、样品用量少，因而，倍受分析工作者的青睐。
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| 关 键 词： | C18-MCM-41 固相微萃取 高效液相色谱 菲 |
| 文章编号： | 1004-1656（2005）05-0700-03 |
| 收稿时间： | 2004-10-14 |
| 修稿时间： | 2004-12-25 |
Using C18-MCM-41as a new Fiber coating in solid-phase microextraction |
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| HUO Jing-Guo,TIAN Rui,MA Qian,DU Xin-zhen,GAO Jin-zhang. Using C18-MCM-41as a new Fiber coating in solid-phase microextraction[J]. Chemical Research and Application, 2005, 17(5): 700-702 |
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| Authors: | HUO Jing-Guo TIAN Rui MA Qian DU Xin-zhen GAO Jin-zhang |
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| Affiliation: | College of Chemistry and Chemical Engineering, Northwest Normal University, Lanzhou 730070, China |
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| Abstract: | The solid-phase microextraction(SPME)using C_(18)-MCM-41 fiber coating coupling with high performance liquid chromatography(HPLC)was applied to the determination of trace of phenanthrene in environment water.The experimental conditions of SPME,.such as extraction time,extraction temperature,desorption time were optimized.The optimized conditions were as below:room temperature,1000r/min of stirring rate,30 min of extraction time and 3min of desorption time,respectively.The proposed method can be used to determine the phenanthrene in environmental water. |
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| Keywords: | C18 - MCM - 41 SPME HPLC Phenanthrene |
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