Synthesis and structure of complex compound Rh(III) of (NH4)2[Rh(NO2)3(NH3)(µ-OH)]2 composition |
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| Authors: | S P Khranenko I A Baidina S A Gromilov |
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| Institution: | (1) A. V. Nikolayev Institute of Inorganic Chemistsry, Siberian Division, Russian Academy of Sciences, Novosibirsk |
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| Abstract: | The crystalline structure of a new compound Rh(III) of (NH4)2Rh(NO2)3(NH3)(µ-OH)]2 composition has been determined. The crystallographic characteristics are H16N10O14Rh2: a = 6.3963(2) Å, b = 9.3701(4) Å, c = 13.6646(5) Å, β = 102.266(1)°, V = 800.28(5) Å3, Z = 2, d calc = 2.432 g/cm3. The distance Rh...Rh in the dimer is 3.200 Å. |
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| Keywords: | rhodium X-ray phase analysis X-ray diffraction analysis crystallochemistry |
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