Crystals from concentrated glyme mixtures. The single-crystal structure of LiClO4 |
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| Authors: | Henderson Wesley A Brooks Neil R |
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| Affiliation: | Department of Chemical Engineering & Materials Science, University of Minnesota, Minneapolis, Minnesota 55455, USA. wesley.henderson@casaccia.enea.it |
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| Abstract: | A procedure for the preparation of high-quality single crystals from concentrated glyme mixtures is presented. Anhydrous single crystals of LiNO(3) and LiClO(4) were prepared in this manner, and the single-crystal structure of LiClO(4) (orthorhombic, Pnma, a = 8.6447(12) A, b = 6.8512(10) A, c = 4.8254(7) A, Z = 4) was determined as an example. This procedure is expected to be widely applicable for not only salts but also a wide range of other materials solvated by glymes. |
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