A new and convenient synthesis of phendiones oxidated by KBrO3/H2SO4 at room temperature |
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| Authors: | Ren Hua Zheng Hai Chang Guo Hua Jiang Jiang Ke Hui Xu Bei Bei Liu Wei Lin Sun Zhi Quan Shen |
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| Affiliation: | a Department of Polymer Science and Engineering, Zhejiang University, Hangzhou 310027, China;b School of Pharmaceutical and Chemical Engineering, Taizhou University, Taizhou 317000, China |
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| Abstract: | A new method is described to synthesize phendione derivatives from 1,10-phenanthrolines using potassium bromate and 60% sulfuric acid as oxidant, which was easily applicable to scale-up. The reaction conditions are mild and the yields are excellent. The target compounds have been characterized by 1H NMR, and IR. |
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| Keywords: | Phendione 1,10-Phenanthroline 3/H2SO4zz')" href=" #" > KBrO3/H2SO4 Synthesis |
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