Deposition of continuous silicalite-1 films on inorganic fibers |
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Institution: | 1. Centre for Marine and Environmental Research (CIMA), University of Algarve, Faro, Portugal;2. Centre of Marine Sciences (CCMAR), University of Algarve, Faro, Portugal |
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Abstract: | Silicalite-fiber composites were prepared by a new method for the synthesis of molecular sieve films. The method consists of two steps: in the first one, the surface charge of the support is reversed by treatment with a cationic polymer solution and a monolayer of negatively charged colloidal molecular sieve seed crystals is adsorbed on the surface. The second step consists of hydrothermal treatment of the support in a molecular sieve precursor solution resulting in the formation of a continuous film of molecular sieve. The method was applied to carbon, ZrO2, Al2O3, mullite, ceramic and pyrex glass fibers. The crystallization of continuous silicalite-1 films on all types of fibers was confirmed by SEM, XRD, FTIR, DTA analyses and BET surface area measurements. |
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