| Ho3+-Yb3+掺杂磷酸盐玻璃陶瓷的制备与发光性能 |
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| 引用本文： | 赵梦洁,邹翔宇,夏宇行,贾文韬,张洪波,邵晶,苏春辉.Ho3+-Yb3+掺杂磷酸盐玻璃陶瓷的制备与发光性能[J].无机化学学报,2019,35(1):95-100. |
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| 作者姓名： | 赵梦洁 邹翔宇 夏宇行 贾文韬 张洪波 邵晶 苏春辉 |
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| 作者单位： | 长春理工大学材料科学与工程学院;长春师范大学 |
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| 基金项目： | 国家“111”工程（No.D17017）和吉林省科技厅重点研究项目（No.20160204027GX）资助。 |
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| 摘 要： | 采用传统熔融法制备了Na_2O-Y_2O_3-P_2O_5-SiO_2前驱体玻璃,并对前驱体玻璃样品进行热处理,成功合成透明磷酸盐玻璃陶瓷。对玻璃陶瓷样品进行XRD分析确定玻璃基质中有Na_(3.6)Y_(1.8)(PO_4)_3晶体析出。讨论了热处理时间对玻璃陶瓷结晶度和晶粒尺寸的影响,确定热处理温度为655℃,热处理时间为2 h。比较Ho~(3+)单掺和Ho~(3+)-Yb~(3+)共掺玻璃陶瓷上转换发光强度,确定Ho~(3+)与Yb~(3+)的最佳掺杂物质的量之比为1∶2。同时讨论了Ho~(3+)-Yb~(3+)之间的能量转移。使用积分球测得样品的上转换发光量子效率。
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| 关 键 词： | 玻璃陶瓷 磷酸盐 Ho3+-Yb3+掺杂 发光 量子效率 |
| 收稿时间： | 2018/9/22 0:00:00 |
| 修稿时间： | 2018/10/15 0:00:00 |
Preparation and Luminescence Properties of Ho3+-Yb3+ Co-doped Phosphate Glass-Ceramics |
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| ZHAO Meng-Jie,ZOU Xiang-Yu,XIA Yu-Hang,JIA Wen-Tao,ZHANG Hong-Bo,SHAO Jing and SU Chun-Hui.Preparation and Luminescence Properties of Ho3+-Yb3+ Co-doped Phosphate Glass-Ceramics[J].Chinese Journal of Inorganic Chemistry,2019,35(1):95-100. |
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| Authors: | ZHAO Meng-Jie ZOU Xiang-Yu XIA Yu-Hang JIA Wen-Tao ZHANG Hong-Bo SHAO Jing and SU Chun-Hui |
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| Institution: | School of Material Science and Engineering, Changchun University of Science and Technology, Changchun 130022, China,School of Material Science and Engineering, Changchun University of Science and Technology, Changchun 130022, China,School of Material Science and Engineering, Changchun University of Science and Technology, Changchun 130022, China,School of Material Science and Engineering, Changchun University of Science and Technology, Changchun 130022, China,School of Material Science and Engineering, Changchun University of Science and Technology, Changchun 130022, China,School of Material Science and Engineering, Changchun University of Science and Technology, Changchun 130022, China and School of Material Science and Engineering, Changchun University of Science and Technology, Changchun 130022, China;Changchun Normal University, Changchun 130032, China |
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| Abstract: | |
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| Keywords: | glass-ceramics phosphate Ho3+-Yb3+ co-doped luminescence quantum efficiency |
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