| Solvothermal Synthesis and Characterization of HgTe Nanoplatelets Using Mercury（I） Source |
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| 作者姓名： | WU Ke-Jun ;WANG Ming-Sheng ;ZOU Jian-Ping ;XU Gang ;DING Tong-Yong ;GUO Guo-Cong ;HUANG Jin-Shun |
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| 作者单位： | State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter The Chinese Academy of Sciences，State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter The Chinese Academy of Sciences，State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter The Chinese Academy of Sciences，State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter The Chinese Academy of Sciences，State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter The Chinese Academy of Sciences，State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter The Chinese Academy of Sciences，State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter The Chinese Academy of Sciences，Fuzhou Fujian 350002 China Graduate School of the Chinese Academy of Sciences Beijing 100039 China，Fuzhou Fujian 350002 China，Fuzhou Fujian 350002 China，Fuzhou Fujian 350002 China，Fuzhou Fujian 350002 China，Fuzhou Fujian 350002 China，Fuzhou Fujian 350002 China |
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| 基金项目： | This project was supported by the NSF for Distinguished Young Scientist of China (20425104), Fujian Key Laboratory of Nanomaterials (2006L2005), and the NSF of Fujian Province (2004J039) |
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| 摘 要： | Mercury telluride （HgTe） nanoplatelets were obtained via a facile solvothermal reaction of mercury（I） chloride and tellurium powder in ethylenediamine （en）. Mercury（I） was first applied as the mercury sources to prepare nanocrystal HgTe; moreover, the proposed mechanism for the fabrication of the sample was discussed in detail. The HgTe nanoplatelets were characterized by powder X-ray diffraction （PXRD）, scanning electron microscopy （SEM）, transmission electron microscopy （TEM）, high-resolution transmission electron microscopy （HRTEM） and Fourier transform infrared spectroscopy （FT-IR）. The absence of IR absorption may render the title nanocrystal useful as an IR transparent material in the region.
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| 关 键 词： | 晶体生长 碲化汞 纳米材料 溶剂热合成 X-射线技术 |
Solvothermal Synthesis and Characterization of HgTe Nanoplatelets Using Mercury(I) Source |
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| WU Ke-Jun,;WANG Ming-Sheng,;ZOU Jian-Ping,;XU Gang,;DING Tong-Yong,;GUO Guo-Cong,;HUANG Jin-Shun.Solvothermal Synthesis and Characterization of HgTe Nanoplatelets Using Mercury(I) Source[J].Chinese Journal of Structural Chemistry,2008,27(4):461-466. |
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| Authors: | WU Ke-Jun WANG Ming-Sheng ZOU Jian-Ping XU Gang DING Tong-Yong GUO Guo-Cong HUANG Jin-Shun |
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| Institution: | [1]State Key Laboratory of Structural Chemistry, Fujian Institute of Research on theStructure of Matter, The Chinese Academy of Sciences, Fuzhou, Fujian 350002, China [2]Graduate School of the Chinese Academy of Sciences, Beijing 100039, China |
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| Abstract: | Mercury telluride (HgTe) nanoplatelets were obtained via a facile solvothermal reaction of mercury(I) chloride and tellurium powder in ethylenediamine (en). Mercury(I) was first applied as the mercury sources to prepare nanocrystal HgTe; moreover, the proposed mechanism for the fabrication of the sample was discussed in detail. The HgTe nanoplatelets were characterized by powder X-ray diffraction (PXRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM) and Fourier transform infrared spectroscopy (FT-IR). The absence of IR absorption may render the title nanocrystal useful as an IR transparent material in the region. |
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| Keywords: | crystal growth mercury telluride nanomaterials solvothermal synthesis X-ray techniques |
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