Hardness-packing density scaling relations for cohesive-frictional porous materials

Recent progress in instrumented nanoindentation makes it possible today to test in situ phase properties and structures of porous materials that cannot be recapitulated ex situ in bulk form. But it requires a rigorous indentation analysis to translate indentation data into meaningful mechanical properties. This paper reports the development and implementation of a multi-scale indentation analysis based on limit analysis, for the assessment of strength properties of cohesive-frictional porous materials from hardness measurements. Based on the separation-of-scale condition, we implement an elliptical strength criterion which results from the nonlinear homogenization of the strength properties of the constituents (cohesion and friction), the porosity and the microstructure, into a computational yield design approach to indentation analysis. We identify the resulting upper bound problem as a second-order conical optimization problem, for which advanced optimization algorithms became recently available. The upper bound yield design solutions are benchmarked against solutions from comprehensive elastoplastic contact mechanics finite element solutions and lower bound solutions. Furthermore, from a detailed parameter study based on intensive computational simulations, we identify characteristic hardness-packing density scaling relations for cohesive-frictional porous materials. These scaling relations which are developed for two pore-morphologies, a matrix-pore morphology and a polycrystal (perfect disordered) morphology, are most suitable for the reverse analysis of the strength parameters of cohesive-frictional solids from indentation hardness measurements.