The crystal and molecular structures of 2-hydroxy-1-naphthalenecarboxaldehyde and 3-hydroxy-2-naphthalenecarboxaldehyde |
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Authors: | Juan M. Fernández-G Georgina Espinosa-Pérez |
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Affiliation: | 1. Instituto de Química. U.N.A.M., Circuito Exterior. Cd. Universitaria, Coyoacán 04510, México, D.F., México
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Abstract: | The crystal and molecular structures of 2-Hydroxy-1-naphthalenecarboxaldehyde (I) and 3-Hydroxy-2-naphthalenecarboxaldehyde (II) were determined. Compound (I) crystallizes in the space groupP21/n witha+5.589(2),b+9.352(2), andc+15.490(3) Å, =98.14(3)°, andZ+4. Compound (II) crystallizes inP21/n witha+16.831(11),b+5.936(3), andc+8.295(3) Å =97.24(5)°. andZ+4. The structures were solved by direct methods, and refined by fullmatrix least squares toR+0.071 andRw+0.083 forI, andR+0.047 andRw+0.061 forII. |
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