Abstract: | Abstract A simple, highly sensitive and selective fluorescence synergistic method has been developed for rapid determination of stilboestrol with Triton × — 100 (λex = 318nm, λem = 415nm) at pH 8.80 ~ 10.20. The calibration graph is linear over the range of 0.0 ~ 30.0μg/10ml. The detection limit is 0.03μg/ml stilboestrol. The method has been successfully applied for the determination of stilboestrol in tabellae stilboestrol and injectio stilboestrol with satisfactory results. It can also be applied for the determination of stilboestrol in body fluid of special patients. |