Synthesis of 3-acetyl-6-(<Emphasis Type="Italic">o</Emphasis>-methyl benzoyl)-<Emphasis Type="Italic">N</Emphasis>-ethylcarbazole |
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| Authors: | Ling Gong Chao Qian Xinzhi Chen |
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| Institution: | 1.Department of Chemical Engineering,Zhejiang University,Hangzhou,People’s Republic of China;2.Engineering Department,ShanghaiChem Engineering Incorporation,Shanghai,People’s Republic of China |
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| Abstract: | 3-Acetyl-6-(o-methyl benzoyl)-N-ethylcarbazole was prepared through successive o-methyl benzoylation and acetylation of N-ethylcarbazole in one pot. The overall yield was 85.6% and the structure was confirmed by 1H-NMR and 13C-NMR. A preliminary investigation had also been carried out on the mechanism of the o-methyl benzoylation of N-ethylcarbazole. |
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