| N,N-二乙基蒎酮酸酰胺合成的研究 |
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| 引用本文： | 金建忠,夏卫华,哈成勇.N,N-二乙基蒎酮酸酰胺合成的研究[J].广州化学,2002,27(2):11-16. |
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| 作者姓名： | 金建忠 夏卫华 哈成勇 |
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| 作者单位： | 1. 浙江树人大学轻工与环保学院,浙江,杭州,310015
2. 中国科学院广州化学研究所,广东,广州,510650 |
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| 摘 要： | 松节油的主要成分α-蒎烯在十二烷基硫酸钠的乳化作用下用高锰酸钾氧化,生成蒎酮酸。研究了氧化过程中各种反应因素的影响,得出较适宜的反应条件,蒎酮酸的收率在60%以上。蒎酮酸经过酰氯化后再和二乙胺反应,合成了可能有生物活性的N,N-二乙基蒎酮酸酰胺。
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| 关 键 词： | 松节油 α-蒎烯 生物活性 |
| 文章编号： | 1009-220(2002)02-0011-06 |
| 修稿时间： | 2001年12月3日 |
The Synthesis of N,N-Diethyl-Pinonic Amide |
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| JIN Jian-zhong,XIA Wei-hua,HA Cheng-yong.The Synthesis of N,N-Diethyl-Pinonic Amide[J].Guangzhou Chemistry,2002,27(2):11-16. |
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| Authors: | JIN Jian-zhong XIA Wei-hua HA Cheng-yong |
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| Institution: | JIN Jian-zhong1,XIA Wei-hua2,HA Cheng-yong*2 |
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| Abstract: | Pinonic acid was synthesized from turpentine, which is abundant in China. Factors that affected the oxidation of alpha-pinene were studied. The better reaction condition was found and the yield of PA was more than 60%. Pinonic acyl chloride was prepared by the reaction of pinonic acid with SOCl2 in the presence of DMF. Pinonic acyl chloride was reacted with diethyl amine to synthesize N,N-diethyl-pinonic amide. |
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| Keywords: | turpentine alpha-pinene biological activity |
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