A bilateral study for the establishment of comparability in the measurement of ethanol in bioethanol fuel using isotope dilution mass spectrometry |
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Authors: | Tang Lin Teo Can Quan Pui Sze Cheow Ting Huang Tong Kooi Lee Hongmei Li Wei Zhang |
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Institution: | 1. Health Sciences Authority, Chemical Metrology Division, Chemical Metrology Laboratory, 1 Science Park Road, #01-05/06, The Capricorn, Singapore Science Park II, Singapore, 117528, Singapore 2. Chemical Metrology and Analytical Science Division, National Institute of Metrology, No. 18 Bei San Huan Dong Lu, Beijing, 100013, People??s Republic of China
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Abstract: | A bilateral comparative study between two metrology institutes was conducted for the determination of ethanol in bioethanol fuel by isotope dilution mass spectrometry. Measurement procedures were independently developed by the Health Sciences Authority (Singapore) and the National Institute of Metrology (People??s Republic of China). The methods used included headspace gas chromatography?Chigh-resolution mass spectrometry, headspace gas chromatography?Cmass spectrometry (GC-MS) and direct injection to GC-MS. An investigation of all potential sources of uncertainty, including a component of uncertainty due to the effect of using different instruments such as gas chromatography?Cflame ionization detector method, commonly adopted for the analysis of organic volatiles, was carried out. The results of the analyses are consistent within the associated measurement uncertainty of each laboratory, reported at approximately 95% confidence level. |
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