Gas chromatographic subsystem for fast on-line concentration profile measurements for advanced distillation column control |
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Authors: | Niels Hald Pedersen Sten Bay Jørgensen |
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Institution: | Process Design, Dynamics and Control Group, Instituttet for Kemiteknik, Technical University of Denmark, DK 2800 Lyngby Denmark |
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Abstract: | An automated gas chromatographic subsystem for the provision of fast and reliable concentration profile data for distillation column control is presented. The subsystem consists of a gas chromatograph, equipment for sample conditioning and a PC/AT compatible computer communicating with the supervisory process computer. A fast separation time is obtained through the use of a liquid chromatographic packing material and a high pressure drop across the column. Preliminary results show separation times below 10 s for the water-methanol-isopropanol system. Peak areas are quantified by use of parameter estimation in the frequency domain, a method that does not demand complete peak separation. |
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Keywords: | Concentration profile measurements Distillation column control Process analysis |
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