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Synthesis of readily cleavable immobilized 1,10-phenanthroline resins
Authors:Slough Greg A  Krchnák Viktor  Helquist Paul  Canham Stephen M
Affiliation:Chemistry Department, Kalamazoo College, 1200 Academy Street, Kalamazoo Michigan 49006, USA. gslough@kzoo.edu
Abstract:1,10-Phenanthroline is derivatized and ultimately immobilized on two different polystyrene/divinylbenzene solid supports using convenient methodology. All syntheses are amenable to semiautomatic processing and are scalable for high-throughput screening. A domino copper-catalyzed coupling-cyclization reaction is used to illustrate applicability in catalytic studies.
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