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Solid-state vibrational spectra and theoretical study of alaninamide acetate |
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| Authors: | T Kolev |
| Institution: | (1) Institute of Organic Chemistry, Bulgarian Academy of Sciences, Acad. G. Bonchev Str. 9, 1113 Sofia, Bulgaria;(2) Faculty of Chemistry, Department of Organic Chemistry, Plovdiv University “P. Hilendarski”, 24 Tzar Assen Str., 4000 Plovdiv, Bulgaria |
| Abstract: | Solid-state IR and Raman spectroscopic elucidation of alaninamide acetate is preformed by means of the possibilities of linear-polarized IR and Raman methods. The experimental assignment is compared with theoretical vibrational analysis with the intention to explain the influence of intermolecular interactions in solid phase on the spectroscopic properties of the compound studied. The 1H and 13C NMR spectra in solution are compared with the corresponding ones of alanine, studying the amidation effect on the chemical shift signals in the alanine moieties. |
| Keywords: | alaninamide acetate IR and Raman spectroscopy solid state IR-LD study vibrational analysis 1H and 13C NMR |
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