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Synthesis and surface structural characteristics of new polysiloxane xerogel
Authors:A S Zasukhin  L K Neudachina  Yu G Yatluk  L V Adamova  V A Osipova  E M Gorbunova  Yu S Moskaleva and T Yu Larina
Abstract:Pyridylethylaminopropylpolysiloxane xerogel (PEAPPSX) was synthesized by sol-gel technology. The composition of the substance was determined via elemental analysis and 1H NMR spectroscopy. The surface structural characteristics of the xerogel were determined by electron microscopy and low-temperature nitrogen sorption; thermal analysis was also performed. It was established that the content of functional groups in PEAPPSX was 2.43 mmol/g, and that xerogel is a mesoporous substance with a developed surface (121.71 m2/g).
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