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Catalyst‐Free One‐Pot Synthesis of Ketene Imines under Ultrasound Irradiation
Authors:Hamideh Emtiazi  Mohammad A Amrollahi
Institution:Department of Chemistry, College of Science, Yazd, University, P.O. Box 89195‐741, Yazd, Iran
Abstract:An efficient and simple procedure for the synthesis of ketene imines via a one‐pot three‐component reaction of cyclohexyl isocyanide, diethyl acetylenedicarboxylate, and 1,4‐dihydropyridines under ultrasonic irradiation is described. The remarkable advantages are the simplicity of the experimental procedures, high yields, and short reaction times.
Keywords:Acetylene esters  Pyridine  1  4‐dihydro‐  Isocyanides  Ketene imine
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