| 2-苯乙烯基喹啉染料的无溶剂微波合成 |
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| 引用本文： | 李凤梅,王兰英,王少康,张祖训. 2-苯乙烯基喹啉染料的无溶剂微波合成[J]. 有机化学, 2004, 24(1): 50-52 |
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| 作者姓名： | 李凤梅 王兰英 王少康 张祖训 |
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| 作者单位： | 西北大学化学系,西安,710069 |
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| 摘 要： | 在微波促进无溶剂条件下,由2-甲基喹啉与取代芳香醛在醋酐作用下合成了一系列2-苯乙烯基喹啉染料,该法操作简便、收率高.经元素分析, 1H NMR, MS, IR和UV确证了产物的结构.
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| 关 键 词： | 微波辐射 苯乙烯染料 2-甲基喹啉 芳香醛 |
| 修稿时间： | 2003-04-14 |
Solvent-Free Synthesis of Styryl Dyes with Quinoline Nucleus Using Microwave Irradiation |
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| LI,Feng-Mei WANG,Lan-Ying WANG,Shao-Kang ZHANG,Zu-Xun. Solvent-Free Synthesis of Styryl Dyes with Quinoline Nucleus Using Microwave Irradiation[J]. Chinese Journal of Organic Chemistry, 2004, 24(1): 50-52 |
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| Authors: | LI Feng-Mei WANG Lan-Ying WANG Shao-Kang ZHANG Zu-Xun |
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| Abstract: | A series of styryl dyes with quinoline nucleus were conveniently synthesized by the reaction of 2-methylquinoline with aromatic aldehydes in the present of Ac 2O under solvent-free microwave irradiation with high yields. The products were identified by 1H NMR, IR, MS, UV-vis and elemental analysis. |
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| Keywords: | microwave irradiation styryl dye 2-methylquinoline aromatic aldehyde |
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