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Crystal structure of a novel two-dimensional supramolecular network based on polyoxoanion and yttriumIII coordination cation |
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| Authors: | He Shuiyang Peng Ke Ning Wei Wang Daqi Shi Qizhen |
| Affiliation: | 1.Department of Chemistry, Northwest University and Shaanxi Key Laboratory of Physico-Inorganic Chemistry, 710069, Xi’an, China ;2.College of Chemistry and Chemical Engineering, Liaocheng University, 252059, Liaocheng, China ; |
| Abstract: | A novel compound (NH4)2Y(H2O)8[PMo10V2O40]·10H2O has been prepared in an aqueous solution and characterized by elemental analysis, IR, and TG-DTG analysis. X-ray diffraction analysis was carried out on (NH4)2Y(H2O)8 [PMo10V2O40]·10H2O single crystal, which crystallizes in the monoclinic system of a space group P21/c witha=0. 9871 (3) nm,b=1. 5424 (5) nm,c=2.7924(9) nm, β = 94.183(5)° and Z=2. In the compound, a two-dimensional network is constructed by the PMo10V2O 5−40 anion and the Y(H2O) 3+8 cation building blocks via hydrogen bonding exhibiting the porous structure. |
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