Preparation of dicyclopentadienylmetal-bis(trimethyl phosphite) complexes of titanium(II) and zirconium(II) by sodium atom reduction |
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| Authors: | M Chang PL Timms RB King |
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| Institution: | School of Chemistry, University of Bristol, Bristol BS8 1TS Great Britain;Department of Chemistry, University of Georgia, Athens, Georgia 30602 U.S.A. |
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| Abstract: | The complexes (C5H5)2MP(OCH3)3]2 (M = Ti and Zr) can be prepared by condensing sodium atoms at ?100°C into tetrahydrofuran solutions containing (C5H5)2MCl2 and excess trimethyl phosphite. |
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