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Cinnamolid‐3β‐ol hemihydrate and 3β‐hydroxycinnamolide acetate,two drimanolide‐class sesquiterpene lactones from Warburgia ugandensis
Authors:Yi‐Xun Zhang  Shauntina H Jackson  Mohamed S Rajab  Frank R Fronczek  Steven F Watkins
Abstract:3β‐Hydr­oxy‐7‐drimen‐12,11‐olide hemihydrate, C15H22O3·0.5H2O, (I), has two sesquiterpene mol­ecules and one water mol­ecule in the asymmetric unit. The OH groups of both mol­ecules and both H atoms of the water mol­ecule are involved in near‐linear inter­molecular hydrogen bonds, having O?O distances in the range 2.632 (3)–2.791 (2) Å. 3β‐Acet­oxy‐7‐drimen‐12,11‐olide, C17H24O4, (II), has its ring system in very nearly the same conformation as the two mol­ecules of (I).
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