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Simple synthesis of quinolines and dibenzo[b,f][1,5]diazocines under microwave irradiation
Authors:Dai-Il Jung  Ju-Hyun Song  Eon-Jin Lee  Yun-Young Kim  Do-Hun Lee  Yong-Gyun Lee  Jung-Tai Hahn
Institution:aDepartment of Chemistry, Dong-A University, Saha-Gu, Busan 604 714, Republic of Korea;bDepartment of Beautycare, Young-Dong University, Chungcheongbuk-do 370 701, Republic of Korea
Abstract:Quinolines 3af, 5a–f, and dibenzob,f]1,5]diazocines 4, 6 were synthesized in the presence of 0.5 equiv. of diphenyl phosphate (DPP) under microwave irradiation. The obtained yield of 6,12-diphenyl-dibenzob,f]1,5]diazocine 4 was higher when using anhydrous DPP than when using HCl, H3PO4, and CH3COOH.
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