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Synthesis and spectroscopic studies of trans-bis-(3,5-dimethyl-4-nitrosopyrazole) dimer
Authors:Zeki A. Nasir Al-Shamkhani
Affiliation:Department of Chemistry, College of Science, University of Basrah, Basrah, Iraq
Abstract:Bis-(3,5-dimethyl-4-nitrosopyrazole) dimer was prepared by reaction of acetyl acetone with nitrous acid and condensation with hydrazine. Spectroscopic techniques, including IR, UV, 1H NMR, and 13C NMR, and CHN analysis were used to identify the product.
Keywords:Nitroso compounds   Heterocyclic dimer   Bis-(3,5-dimethyl-4-nitrosopyrazole) dimer   Semi-empirical AM1 and PM3 methods
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