A simple approach to benzothiazoles from 2-chloronitrobenzene,elemental sulfur,and aliphatic amine under solvent-free and catalyst-free conditions |
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| Authors: | Yao Tong Qiang Pan Zengqiang Jiang Dazhuang Miao Xuesong Shi Shiqing Han |
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| Affiliation: | 1. College of Biotechnology and Pharmaceutical Engineering, Nanjing Tech University, Nanjing 211816, China;2. Key Laboratory of Synthetic Chemistry of Natural Substances, Shanghai Institute of Organic Chemistry, CAS, 345 Lingling Road, Shanghai 200032, China |
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| Abstract: | A novel solvent-free and catalyst-free synthesis of benzothiazoles from 2-chloronitrobenzene, elemental sulfur, and aliphatic amine has been developed. The reaction tolerated a wide range of functionalities, and various benzothiazoles were synthesized in moderate to good yields in the absence of external oxidant or reductant. |
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| Keywords: | Benzothiazoles 2-Chloronitrobenzene Sulfur Aliphatic amine Catalyst-free |
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