| 2,4,6-三（羟甲基）间二甲苯的合成与表征 |
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| 引用本文： | 贺忠玉,林原斌.2,4,6-三（羟甲基）间二甲苯的合成与表征[J].光谱实验室,2011,28(2):595-597. |
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| 作者姓名： | 贺忠玉 林原斌 |
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| 作者单位： | 湘潭大学化学学院,环境友好化学与应用省部共建教育部重点实验室,湖南省湘潭市雨湖区羊牯塘卢家滩27号,411105 |
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| 基金项目： | 国家自然科学基金资助项目 |
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| 摘 要： | 以间二甲苯为原料,经氯甲基化、酯化、再水解成功制得新物质2,4,6-三（羟甲基）间二甲苯。利用FTIR、1H NMR、13C NMR等手段对产物的结构进行了表征。以间二甲苯计,三步反应的总收率达57.6%。
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| 关 键 词： | 间二甲苯 氯甲基化 羟甲基 合成 |
Synthesis and Characterization of 2,4,6-Tri(Hydroxymethyl)-m-Xylene |
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| HE Zhong-Yu,LIN Yuan-Bin.Synthesis and Characterization of 2,4,6-Tri(Hydroxymethyl)-m-Xylene[J].Chinese Journal of Spectroscopy Laboratory,2011,28(2):595-597. |
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| Authors: | HE Zhong-Yu LIN Yuan-Bin |
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| Institution: | HE Zhong-Yu LIN Yuan-Bin(College of Chemistry,Key Laboratory of Environmentally Friendly Chemistry and Application of Ministry of Education,Xiangtan University,Xiangtan,Hunan 411105,P.R.China) |
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| Abstract: | 2,4,6-tri(hydroxymethyl)-m-xylene was prepared from m-xylene via chloromethylation,esterification and hydrolysis.The structure of the compound was confirmed by FTIR,1H NMR and 13C NMR etc.The overall yield was 57.6%. |
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| Keywords: | m-Xylene Chloromethylation Hydroxymethyl Synthesis |
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