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Radiochemical neutron activation determination of phosphorus in high pure germanium
Authors:V. P. Kolotov  I. I. Sadykov  N. N. Dogadkin  N. N. Nekrasova
Affiliation:(1) V. I. Vernadsky Institute of Geochemistry and Analytical Chemistry, USSR Academy of Sciences, Moscow, (Russia);(2) Institute of Nuclear Physics, Academy of Sciences Uzbek, Tashkent, (Uzbek)
Abstract:A radiochemical procedure for determination of ultra low concentrations of phosphorus in germanium has been developed. The method involves application of multicells autoclaves for matrix distillation and extraction chromatography with dioctyltin diacetate for final phosphorus purification. The detection limit is 40 ppt for a 1-g sample.
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