| 电沉积-烧结法制备Y2O3:Eu 荧光薄膜的研究 |
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| 引用本文： | 曾冬铭,舒万艮,史菲菲. 电沉积-烧结法制备Y2O3:Eu 荧光薄膜的研究[J]. 影像科学与光化学, 2006, 24(2): 126-132. DOI: 10.7517/j.issn.1674-0475.2006.02.126 |
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| 作者姓名： | 曾冬铭 舒万艮 史菲菲 |
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| 作者单位： | 中南大学,化学化工学院,湖南,长沙,410083;中南大学,化学化工学院,湖南,长沙,410083;中南大学,化学化工学院,湖南,长沙,410083 |
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| 摘 要： | 平板显示是显示技术发展的方向,发光材料的薄膜化是显示技术发展的重要研究对象.本研究采用电沉积-烧结方法制备出了氧化钇铕红色荧光薄膜.在0.1 mol/L硝酸钇溶液中加入4%(摩尔分数)0.1 mol/L硝酸铕掺杂,用三电极体系进行阴极电沉积,工作电极的电位为-1.2 V(相对于Ag/AgCl电极),温度65℃,沉积时间为400 s,500℃灼烧2 h,制备出的发光薄膜与高温固相法制备的薄膜对比,其发射光谱的峰位相同.XRD检测显示经不同温度灼烧后,随温度的升高,氧化钇晶相逐渐完整.经SEM扫描,薄膜沉积均匀平整.
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| 关 键 词： | 电沉积-烧结法 薄膜 氧化钇铕 荧光 |
| 收稿时间： | 2005-10-20 |
The Research of the Luminescence Film of Y2O3:Eu Preparated by Method of Electrodeposition-Sinter |
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| ZENG Dong-ming,SHU Wan-gen,SHI Fei-fei. The Research of the Luminescence Film of Y2O3:Eu Preparated by Method of Electrodeposition-Sinter[J]. Imaging Science and Photochemistry, 2006, 24(2): 126-132. DOI: 10.7517/j.issn.1674-0475.2006.02.126 |
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| Authors: | ZENG Dong-ming SHU Wan-gen SHI Fei-fei |
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| Affiliation: | College of Chemistry and Chemical Engineering, Central South University, Changsha 410083, Hunan, P. R. China |
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| Abstract: | The flat panel display is the development direction of display technology.Filming luminescence material possess important position in display technology.In this paper,electrochemical deposition of red luminescent Y_2O_3∶Eu thin films on transparent conducting optically(ITO) glass substrates by cathodic reduction of yttrium nitric has been investigated.Y(OH)_3 deposits were obtained using a conventional three electrode cell that potential of work electrode was-1.2 V vs.Ag/AgCl electrode for 400 s in a 0.1 mol/L Y(NO)_3,with 4%(mol/mol) Eu(NO)_3,temperature 65 ℃.Then the glass coated Y(OH)_3 containing Eu sintered for 2 h at 500 ℃.The luminescence spectrum of film preparated by this method was similar compared with that of the powder preparated by solid methed.XRD confirms the formation of Y_2O_3 and SEM reveal uniformity of film. |
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| Keywords: | electrodeposition-sinter method film Y_2O_3∶Eu luminescence |
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