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Crystal structure of N,N-disalicylidene-(R,S)(S,R)-1,2-ethanediamine |
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| Authors: | A Ramazani L Dolatyari A Morsali V T Yilmaz O Büyükgüngör |
| Institution: | 1. Department of Chemistry, Islamic Azad University-Zanjan Branch, P.O. Box 49195-467, Zanjan, Iran 2. Department of Chemistry, Faculty of Sciences, Tarbiat Modares University, P.O. Box 14115-175, Tehran, Iran 3. Department of Chemistry, Faculty of Arts and Sciences, Ondokuz Mayis University, Kurupelit, Samsun, Turkey 4. Department of Physisc, Faculty of Arts and Sciences, Ondokuz Mayis University, Kurupelit, Samsun, Turkey |
| Abstract: | N,N-disalicylidene-(R,S)(S,R)-1,2-ethanediamine crystallizes in orthorhombic space group Pbca with a = 9.5634(6), b = 14.2917(9), c = 16.9181(8) Å and Z = 4. The crystal structure was solved by direct methods and refined by full-matrix least squares to final values R1 = 0.0 + 399 and wR2 = 0.1004 with 2755 reflections (I > 2σ(I)). The N,N-disalicylidene-(R,S)(S,R)-1,2-ethanediamine molecules exhibit intramolecular N-H...O and are connected by C-H...O and C-H...π interactions to form a 2D supramolecular network. |
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