| 清除树脂辅助液相合成N-苯基高邻苯酞酰亚胺衍生物及其除草活性研究 |
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| 引用本文： | 程辟,任叶果,黄路,胡礼,徐满才,黄明智.清除树脂辅助液相合成N-苯基高邻苯酞酰亚胺衍生物及其除草活性研究[J].合成化学,2005,13(2):130-133,140. |
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| 作者姓名： | 程辟 任叶果 黄路 胡礼 徐满才 黄明智 |
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| 作者单位： | 湖南师范大学,化学化工学院,湖南,长沙,410081;湖南化工研究院,湖南,长沙,410007;湖南化工研究院,湖南,长沙,410007;中南大学,化学化工学院,湖南,长沙,410083 |
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| 基金项目： | SupportedbytheNationalNaturalScienceFoundationofChina(20372021)，NaturalScienceFoundationofHunanProvince(03JJY3018) |
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| 摘 要： | 通过清除树脂辅助液相合成法合成了9个N-苯基高邻苯酞酰亚胺衍生物，纯度70％～95％。其结构经。HNMR，IR，MS和元素分析确认。初步除草活性测试表明部分化合物在150g．ai．ha^-1对苘麻、马刺苋、凹头苋等表现出除草活性。
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| 关 键 词： | 清除树脂 液相合成 原卟啉原氧化酶抑制剂 除草活性 |
Scavenger Resin Assisted Solution-phase Synthesis of N-phenylhomoph-thalimide Derivatives and Study on Their Herbicidal Activities |
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| CHENG Pi,REN Ye-guo,HUANG Lu,Hu Li,XU Man-cai,HUANG Ming-zhi.Scavenger Resin Assisted Solution-phase Synthesis of N-phenylhomoph-thalimide Derivatives and Study on Their Herbicidal Activities[J].Chinese Journal of Synthetic Chemistry,2005,13(2):130-133,140. |
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| Authors: | CHENG Pi REN Ye-guo HUANG Lu Hu Li XU Man-cai HUANG Ming-zhi |
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| Abstract: | Nine N-phenylhomophthalimide derivatives with the purities of 70%～95% were synthesized via solution-phase synthesis utilizing scavenger resin. The structures were confirmed by 1H NMR, IR, MS and elemental analysis. The preliminary herbicidal tests showed that some of the compounds exhibited herbicidal activity to Abutilon avicennae, Portulaca oleracea, Amaranthus spinosus at 150 g.ai·ha-1. |
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| Keywords: | scavenger resin solution-phase synthesis protox inhibitor herbicidal activity |
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