Rapid analysis of cyanuric acid in swimming pool waters by high performance liquid chromatography using porous graphitic carbon |
| |
Authors: | R Cantú O Evans M L Magnuson |
| |
Institution: | (1) National Exposure Research Laboratory, Office of Research and Development, United States Environmental Protection Agency, 26 West Martin Luther King, 45268 Cincinnati, OH, USA;(2) National Risk Management Research Laboratory, Office of Research and Development, United States Environmental Protection Agency, 26 West Martin Luther King, 45268 Cincinnati, OH, USA |
| |
Abstract: | Summary An approach is presented for reducing analysis times of cyanuric acid in swimming pool waters by high performance liquid chromatography
(HPLC). The HPLC method exploits the unique selectivity of porous graphitic carbon (PGC) to fully resolve cyanuric acid from
other pool interferences within 10 min. By carefully timing the injections, multiple injections can be made before the end
of the initial chromatographic run, more than doubling sample throughout. The method utilizes 95% of a 50 mM phosphate buffer
solution (pH 9.1) and 5% methanol (v/v) with UV detection at 213 nm. This approach yielded run times rivaling those of the
fastest methods using silica columns, and with the benefits of increased sensitivity. |
| |
Keywords: | Column liquid chromatography Porous Graphitic Carbon Cyanuric Acid Swimming poole water |
本文献已被 SpringerLink 等数据库收录! |
|