A contribution to the volumetric electrometric determination of some organic peroxides in alkaline media |
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Authors: | J Doležal M Roušal J Zima |
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Institution: | Department of Analytical Chemistry, Faculty of Natural Sciences, Charles University, Albertov 2030, 128 40 Prague 2, Czechoslovakia |
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Abstract: | Conditions for the determination of DBP, CHP, MEKP, and MCHP, as well as m-chloroperbenzoic acid, with a standard solution of SnII-glyc or SnII-sorb by the potentiometric, bipotentiometric, and biamperometric method were found. Quite good results were obtained in comparison with individual modifications of the iodometric method. Large positive errors were found only for the determination of m-chloroperbenzoic acid with SnII-glyc. The reductometric procedure is an advantage in the determination of organic peroxides by this procedure. |
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