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Isolation and X-ray crystal structure of a stable calix[4]arene monohemiketal |
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| Authors: | Peter Timmerman Sybolt Harkema Gerrit J. Van Hummel Willem Verboom David N. Reinhoudt |
| Affiliation: | (1) Laboratory of Organic Chemistry, University of Twente, P.O. Box 217, 7500 AE Enschede, the Netherlands;(2) Laboratory of Chemical Physics, University of Twente, P.O. Box 217, 7500 AE Enschede, the Netherlands |
| Abstract: | The formation of a stable calix[4]arene monohemiketal is described. X-ray crystallographic data provide conclusive evidence for the presence of a stabilizing hydrogen bond.Supplementary Data. Lists of H-atom parameters and bond lengths and angles involving hydrogens have been deposited with the British Library Document Supply Centre as Supplementary Publication No. SUP 82159 (5 pp.). |
| Keywords: | calix[4]arene oxidation hemiketal |
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