| 咪唑-4,5-二羧酸衍生物的合成 |
| |
| 引用本文： | 赵振,李荣清,李燕,张敏.咪唑-4,5-二羧酸衍生物的合成[J].淮阴师范学院学报(自然科学版),2011,10(5):423-425. |
| |
| 作者姓名： | 赵振 李荣清 李燕 张敏 |
| |
| 作者单位： | 1. 淮阴师范学院化学化工学院,江苏淮安,223300
2. 淮阴师范学院化学化工学院,江苏淮安223300／宁夏大学化学化工学院,宁夏银川750021 |
| |
| 基金项目： | 教育部留学回国人员科研启动基金(2008-890);淮安市科技支撑计划工业项目(HAG08040) |
| |
| 摘 要： | 研究了以1H-咪唑-4,5-二羧酸（1）为原料合成1H-咪唑-4,5-二甲酸乙酯（2）和1H-咪唑-4,5-二酰胺（3）的方法和条件,初步考察了催化剂、反应时间、物料比等因素对反应和产率的影响.产品结构经1HNMR、IR和MS表征.
|
| 关 键 词： | 1H-咪唑-4 5-二甲酸乙酯 1H-咪唑-4 5-二酰胺 合成 |
Synthesis of Imidazole-4,5-dicarboxylic Scid Derivatives |
| |
| ZHAO Zhen,LI Rong-qing,LI Yan,ZHANG Min.Synthesis of Imidazole-4,5-dicarboxylic Scid Derivatives[J].Journal of Huaiyin Teachers College(Natrual Science Edition),2011,10(5):423-425. |
| |
| Authors: | ZHAO Zhen LI Rong-qing LI Yan ZHANG Min |
| |
| Institution: | 1,2(1.School of Chemistry and Chemical Engineering,Huaiyin Normal University,Huaian Jiangsu 223300,China)(2.School of Chemistry and Chemical Engineering,Ningxia University,Yinchuan Ningxia 750021,China) |
| |
| Abstract: | The synthetic methods and conditions of diethyl 1H-imidazole-4,5-dicarboxylate(2) and 1H-imidazole-4,5-dicarboxamide(3) were studied using 1H-imidazole-4,5-dicarboxylic acid(1) as a starting material.Influence of catalysts,reaction time and amounts of reactants on yields of products was preliminarily investigated.Compounds 2 and 3 were characterised by 1H NMR、IR and MS. |
| |
| Keywords: | diethyl 1H-imidazole-4 5-dicarboxylate 1H-imidazole-4 5-dicarboxamide synthesis |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
