Synthesis of 1,10-dimethylbicyclo[8.8.8]hexacosane and 1,10-dihydroxybicyclo[8.8.8]hexacosane |
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| Authors: | Jones Ian W Monguchi Yasunari Dawson Alice Carducci Michael D Mash Eugene A |
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| Affiliation: | Department of Chemistry, University of Arizona, Tucson, 85721-0041, USA. |
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| Abstract: | [structure: see text] 1,10-Dimethylbicyclo[8.8.8]hexacosane (1) and 1,10-dihydroxybicyclo[8.8.8]hexacosane (2) were prepared in 4% yield over seven steps and in 18% yield over three steps, respectively, starting from 1,10-cyclooctadecanedione. The identities and out,out conformations of these compounds were established by single-crystal X-ray analysis. |
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