Synthesis of bis(diethyldithiocarbamato)manganese(II) and tris(diethyldithiocarbamato)manganese(III) |
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Authors: | Cassandra T Eagle Grant N Holder Amanda B Goodman Patrick E Hicks Katherine P Shaber |
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Institution: | (1) Department of Chemistry, Appalachian State University, Boone, NC, 28608 |
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Abstract: | An ideal undergraduate introduction to the challenges of synthesis and characterization of air-sensitive compounds is accomplished in the preparation of bis(diethyldithiocarbamato)manganese(II). This economical experiment employs a glovebag, low-cost and low-toxicity chemicals, and is completed in one undergraduate laboratory period. For comparison purposes, the synthesis and characterization of air-stable tris(diethyldithiocarbamato)manganese(III) is also described. |
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