Electroorganic synthesis of 6-aminonicotinic acid from 2-amino-5-chloropyridine |
| |
| Authors: | R. Ramesh RajuS. Krishna Mohan S. Jayarama Reddy |
| |
| Affiliation: | Electrochemical Research Laboratories, Department of Chemistry, Sri Venkateswara University, Tirupati 517502, India |
| |
| Abstract: | A synthesis of 6-aminonicotinic acid by electrochemical hydrogenation of 5-chloro-2-nitropyridine and electrochemical carboxylation of 2-amino-5-chloropyridine at a cathode surface in the presence of sulphuric acid and carbon dioxide in a dimethylformamide (DMF) solution at an apparent current density of 10 mA/cm2 using an undivided cell with good yields is reported. |
| |
| Keywords: | 6-aminonicotinic acid 5-chloro-2-nitropyridine 2-amino-5-chloropyridine electroorganic synthesis |
| 本文献已被 ScienceDirect 等数据库收录！ |
