| 尾式卟啉-5-氟尿嘧啶及其金属络合物的光谱分析 |
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| 引用本文： | 杨秋青,韩士田,张慧娟.尾式卟啉-5-氟尿嘧啶及其金属络合物的光谱分析[J].分析化学,2001,29(12):1379-1383. |
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| 作者姓名： | 杨秋青 韩士田 张慧娟 |
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| 作者单位： | 河北师范大学实验中心化学系, |
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| 摘 要： | 合成了24种新型的尾式卟啉-5-氟尿嘧啶化合物及其金属锰络合物，通过核磁共振氢谱（NMR）、质谱（MS）、红外光谱（IR）、紫外光谱（UV）及元素分析确定了其结构，并讨论了24种化合物光谱的关系特征及其规律，确定卟啉类配体与金属络合的NMR、IR、UV判据。
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| 关 键 词： | 尾式卟啉 5－氟尿嘧啶 金属锰 核磁共振氢谱 红外光谱 紫外光谱 络合物 分析 抗癌活性 抗代谢药物 |
Spectral and Antitumor Activity Studies of Tail-porphyin-5-fluorouracil and Their Metallic Manganese Complexes |
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| Abstract: | kinds of novel 5 fluorouracil porphyrin were synthesized. Their structures have been confirmed by 1H nuclear magnetic resonance (NMR), infrared (IR), ultraviolet (UV), mass spectrometry (MS) and elemental analysis. The spectral characteristics and chemical shift change regulation of 24 compounds were discussed. 1HNMR, IR, UV data for these compounds have been systematically summarized and can be used to facilitate structural interpretation of similar compounds. |
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| Keywords: | Tail porphyin 5 fluorouracil manganese 1H nuclear magnetic resonance infrared ultraviolet antitumor activity |
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