| 以2-(4′-氯苯甲酰基)苯甲酸及联吡啶为配体的锌、钴两个链状配合物的合成及晶体结构 |
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| 引用本文： | 李秀梅,牛艳玲,王志涛.以2-(4′-氯苯甲酰基)苯甲酸及联吡啶为配体的锌、钴两个链状配合物的合成及晶体结构[J].无机化学学报,2011,27(8):1659-1663. |
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| 作者姓名： | 李秀梅 牛艳玲 王志涛 |
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| 作者单位： | 通化师范学院化学系,通化,134002 |
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| 基金项目： | 吉林省教育厅科学技术研究项目(No.2011.459)资助 |
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| 摘 要： | 通过水热法合成了2个新的配合物Zn(cbba)2(bipy)0.5]n(1)和Co(cbba)2(bipy)(H2O)2]n(2)(Hcbba=2-(4′-氯-苯甲酰基)苯甲酸，bipy=4，4′-联吡啶)。并对其进行了元素分析、红外光谱、热重和X-射线单晶衍射测定。它们都呈现一维链状结构。
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| 关 键 词： | 水热合成 晶体结构 配合物 |
Synthesis and Crystal Structure of Two Chain-Like Complexes of Znic,Cobalt with 2-(4'-Chlorine-benzoyl)benzoic Acid and Bipyridine Ligands |
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| LI Xiu-Mei,NIU Yan-Ling and WANG Zhi-Tao.Synthesis and Crystal Structure of Two Chain-Like Complexes of Znic,Cobalt with 2-(4'-Chlorine-benzoyl)benzoic Acid and Bipyridine Ligands[J].Chinese Journal of Inorganic Chemistry,2011,27(8):1659-1663. |
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| Authors: | LI Xiu-Mei NIU Yan-Ling and WANG Zhi-Tao |
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| Institution: | Department of Chemistry, Tonghua Teachers College, Tonghua, Jilin 134002, China,Department of Chemistry, Tonghua Teachers College, Tonghua, Jilin 134002, China and Department of Chemistry, Tonghua Teachers College, Tonghua, Jilin 134002, China |
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| Abstract: | Two new complexes Zn(cbba)2(bipy)0.5]n (1) and Co(cbba)2(bipy)(H2O)2]n (2) (Hcbba=2-(4'-chlorinebenzoyl)benaoic acid,bipy=4,4'-bipyridine) have been hydrothermally synthesized and structurally characterized by elemental analysis,IR,TG and single-crystal X-ray diffraction.They all exhibit one-dimensional chain-like structure.CCDC:824487,1 ; 824486,2. |
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| Keywords: | hydrothermal synthesis crystal structure complex |
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