Determination of trace iron in high purity sodium fluoride by graphite furnace atomic absorption spectrometry |
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Authors: | Qian Sha-hua Huang Gan-quan Xue Ai-fang Chen Li-hua Wang Mei-lin |
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Affiliation: | (1) College of Chemistry and Environmental Science, Wuhan University, 430072 Wuhan, China |
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Abstract: | A method is described for the direct determination of iron in high purity sodium fluoride using graphite furnace atomic absorption spectrometry. Interferences caused by the matrix are investigated. It is shown that the ashing temperature can be increased to 1 400°C and matrix interferences eliminated, the sensitivity of iron increased in 1. 27 fold by the addition of nickel nitrate. The method is applied to the determination of iron in sodium fluoride and satisfactory results are obtained. Biography: QIAN Sha-hua (1954-), female, associate professor |
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Keywords: | Graphite furnace atomic absorption spectrometry iron determination sodium fluoride matrix modifier |
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