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Residue Analysis of Oxytetracycline in Water and Sediment Samples by High-Performance Liquid Chromatography and Immunochemical Techniques
Authors:Markus Himmelsbach  Wolfgang Buchberger
Affiliation:(1) Department of Analytical Chemistry, Faculty of Chemistry, University of Murcia, E-30071 Murcia, Spain
Abstract:A simple photochemical method for the determination of ethanol using a flow-injection system is proposed. The method is based on the photo-oxidation of ethanol in the presence of UO22+ and Fe3+ upon irradiation with visible light. The Fe2+ produced in the photochemical process was monitored by measuring the absorbance after complexation with ferrozine. The range of measurements depended on the length of the irradiation time. The sample throughput was 60 samples h–1. The usefulness of the method was demonstrated by determining ethanol levels in different beverages.
Keywords:: Ethanol   photochemical reaction   flow-injection   spectrophotometry.
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