A Convenient Synthesis of 2-Oxazolines and 2-Benoxazoles with PPh3-DDQ as the Dehydrating Reagent |
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Authors: | Quancai Xu Zhengning Li Huiying Chen |
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Affiliation: | 1. College of Environmental and Chemical Engineering, Dalian University, Dalian, Liaoning 116622, China;2. Liaoning Key Laboratory of Bioorganic Chemistry, Dalian University, Dalian, Liaoning 116622, China;3. College of Life Science, Dalian Nationalities University, Dalian, Liaoning 116605, China |
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Abstract: | 2‐Oxazolines and 2‐benoxazoles were synthesized in high yields from acylamino alcohols and acylamino‐ phenols, respectively, with triphenylphosphine‐2,3‐dichloro‐5,6‐dicyanobenzoquinone (PPh3‐DDQ) as the dehydrating and activating reagent. The synthesis was accomplished under neutral conditions. |
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Keywords: | oxazoline benzoxazole synthesis dehydrative cylization 2,3‐dichloro‐5,6‐dicyanobenzoquinone triphenylphosphine |
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