Regioselective synthesis and structural elucidation of 1,4-disubstituted 1,2,3-triazole derivatives using 1D and 2D NMR spectral techniques |
| |
Authors: | Babu Thelagathoti Hari Kumar B V N Phani Rajeswari C Perumal Paramasivan T |
| |
Affiliation: | 1. Organic Chemistry Division, Central Leather Research Institute, , Adyar, Chennai, 600 020 India;2. Chemical Physics Laboratory, Central Leather Research Institute, , Adyar, Chennai, 600 020 India |
| |
Abstract: | Regioselective synthesis of 2-[1-(2-oxo-2-phenylethyl)-1H-[1,2,3]triazol-4-ylmethoxy]-benzaldehyde derivatives was achieved by [3 + 2] cycloaddition reaction of 2-(prop)-2-ynyloxy-benzaldehyde derivatives with phenacyl azide. The regiochemistry and the spectral assignments of the synthesized triazole derivatives were studied using both 1D and 2D NMR spectral techniques in solution. |
| |
Keywords: | 1H NMR 13C NMR 2D NMR 1,4‐disubstituted 1,2,3‐triazoles |
本文献已被 PubMed 等数据库收录! |
|