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N2O-C2H2火焰原子吸收光谱法测定电化学浸渍液中的钴
引用本文:薛光荣,夏敏勇.N2O-C2H2火焰原子吸收光谱法测定电化学浸渍液中的钴[J].化学分析计量,2006,15(4):21-23.
作者姓名:薛光荣  夏敏勇
作者单位:1. 上海空间电源研究所,上海,200233
2. 上海安谱科学仪器有限公司分析测试中心,上海,200030
摘    要:运用N2O-C2H2火焰原子吸收光谱法测定电化学浸渍液中的钴含量。通过试验确定了共振线、燃烧器高度、灯电流、酸性介质、火焰等实验条件。用该方法对样品中钴含量进行分析,测定结果的相对标准偏差小于1.0%(n=6),加标回收率为97.3%~98.8%。该方法适用于电化学浸渍液中钴含量的控制分析和样品系统分析。

关 键 词:N2O-C2H2火焰  原子吸收光谱法  电化学浸渍液  
修稿时间:2006年4月11日

DETERMINATION OF COBALT IN BATTERY IMPREGNATING SOLUTION BY N2O-C2H2 FLAME ATOMIC ABSORPTION SPECTROMETRY
Xue Guangrong,Xia Minyong.DETERMINATION OF COBALT IN BATTERY IMPREGNATING SOLUTION BY N2O-C2H2 FLAME ATOMIC ABSORPTION SPECTROMETRY[J].Chemical Analysis And Meterage,2006,15(4):21-23.
Authors:Xue Guangrong  Xia Minyong
Abstract:Cobalt content in battery impregnating solution was determined by N_(2)O-C_(2)H_(2) flame atomic absorption spectrometry.The resonance line,burner height,filament current,acid media and flame for the experiment were determined.The relative standard deviation was less than 1.0%(n=6) for the determination of cobalt.The recoveries were 97.3%-98.8%(n=6).The method could be applied to control analysis of cobalt content in battery impregnating solution.
Keywords:N_(2)O-C_(2)H_(2) flame  atomic absorption spectrometer  battery impregnating solution  cobalt
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