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Mercury selenide nanorods: Synthesis and characterization via a simple hydrothermal method
Authors:Mehdi BazarganipourMinoo Sadri  Fatemeh DavarMasoud Salavati-Niasari
Affiliation:a Department of Inorganic Chemistry, Faculty of Chemistry, University of Kashan, Kashan, P.O. Box 87317-51167, Iran
b Department of Chemistry, College of Science, Bu-Ali Sina University, P.O. Box 4135, Hamadan 65174, Iran
c Institute of Nano Science and Nano Technology, University of Kashan, Kashan, P.O. Box 87317-51167, Iran
Abstract:HgSe nanorods have been synthesized through a simple hydrothermal reduction approach. The nanorods formed were ≈45 nm average diameter and ≈3 μm nm in length. X-ray diffraction characterization suggested that the product consists of cubic phase pure HgSe. The as-prepared products were also characterized by scanning electron microscopy (SEM) and transmission electron microscopy (TEM). An X-ray energy dispersive spectroscopy (EDX) study further confirmed the composition and purity of the product. The synthesis procedure is simple and uses less toxic reagents than the previously reported methods. The results showed that the capping agent CTAB (cetyltrimethylammoniumbromide) plays a crucial role in the process. Other factors, such as the reaction time, temperature, different capping agent and the reductant type also have an influence on the morphology of the final products to some extent.
Keywords:Hydrothermal   HgSe nanorods   Co-precipitation   Solution-chemical
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